You may use the following procedure to validate the setting temperature, ranging from 282K-330K. Temperature correction is routinely checked by the facility Note that temperature correction is usually being enabled which should not be altered by users.
- Load the 99.8% Methanol-d4 Bruker reference sample.
- Lock on Methanol-d4.
- Do a round of "topshim"
- create a zg30 experiment set; Click on "getprosol" icon to use default pulse length and power level; Set ds=0, ns=1, rg=1.
- Type "zg" to run the experiment, and then "apk" to process the data.
- type "calctemp D" to obtain the calculated probe temperature. Ideally the calculated temperature should be very close to the settting temperature.