Students and a professor performing research with lasers.

1H-13C HSQC

Tutorial link

  1. Hsqcetgp data

    Go to an existing experiment (pulse program: hsqcetgp), type “edc” to copy its parameters and generate a new experiment number. Or in an new experiment number "rpar HSQCETGP".

  2. Type “eda”, set parameters td, ns, sw, O1P and O2P, CNST2. Note that CNST2 can be different for different C-H bond.

  3. Type “ased” to adjust power length and power level for both 1H and 13C, including p1, pL1, p3, pL2, pL12, and pcpd2. Or type "getprosol 1H A B" to set power related parameters. A is the pulse length in µs, and B is the power leverl in dB.

  4. Start the experiment by rga and zg; Process the FID by typing “xfb”. Phase the spectrum when necessary.

Spectrum data